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Total No of Questions: 8
Total No. of Printed Pages: 2
Roll No
MPH-101T
M.Pharmacy (PCI), I Semester
Examination, December 2023
Modern Pharmaceutical Analytical Techniques
Time: Three Hours
Maximum Marks: 70
Note: i) Attempt any five questions out of eight.
ii) All questions carry equal marks.
1.
a) Define chromatography? Enlist different types of chromatographic techniques. Write the principle of thin layer chromatography.
b) Discuss stationary phase and mobile phase of Affinity Chromatography
2.
a) Describe Thermal Conductivity Detector and Flame Ionization Detector.
b) Explain Instrumentation of Atomic absorption spectroscopy
3.
a) Discuss the terms in detail: Spin-Spin Coupling and Coupling constant.
b) What is fluorescence Quenching? Discuss its importance.
4.
a) Discuss Laws and Instrumentation associated with UV-Visible spectroscopy.
b) Enumerate UV detectors and explain Photo Multiplier Tube in detail.
5.
a) How will you differentiate between Acetaldehyde and acetylene of compounds using IR spectroscopy?
b) Write detail note on FT technique of IR spectroscopy
6.
a) Discuss in detail on X ray diffraction methods and Braggs law.
b) How Bragg's law applied on X-ray diffraction. Discuss X-ray sources.
7.
a) Define electrophoresis? Discuss various types of electrophoresis in details.
b) Describe the principle of atomic absorption spectroscopy. Discuss atomization techniques used.
8.
Write Short note on any two:
a) Auxochrome and Shielding effect
b) Merits and Demerits of Gas Chromatography
c) Mc-Lafferty Rearrangement
d) Isotopic Abundance